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Author
Zarr, R. R. | Flynn, D. R. | Hettenhouser, J. W. | Brandenburg, N. J. | Healy, W. M.
Title
Fabrication of a Guarded-Hot-Plate Apparatus for Use Over an Extended Temperature Range and in a Controlled Gas Atmosphere.
Coporate
National Institute of Standards and Technology, Gaithersburg, MD MetSys Corp., Millwood, VA
Sponsor
North American Insulation Manufacturers Association DOE Office of Industrial Technology
Book or Conf
International Thermal Conductivity 28th Conference/International Thermal Expansion 16th Symposium. Proceedings. June 26-29, 2005, DEStech Publications, Inc., New Brunswick, Canada, Dinwiddie, R.; White, M. A.; McElroy, D. L., Editors, 235-245 p., 2005
Keywords
guarded-hot-plate apparatus | insulation | temperature range | gas atmosphere | transmission | equipment | thermometers | thermocouples | thermopile | calibrating | vaccum chambers
Identifiers
Standard Platinum Resistance Thermometers (SPRTs); metal-sheathed heaters, thermocouples, thermopiles; cold plate assembly; dge guard assembly
Abstract
This paper describes a guarded-hot-plate apparatus suitable for determining the steady-state thermal transmission properties of insulation specimens from 90 K to 900 K in a controlled gas atmosphere from 10-5 kPa to 105 kPa. The apparatus accommodates flat-slab specimens 500 mm in diameter and from 13 mm to 100 mm in thickness. Fabrication and assembly details are presented for the apparatus hot and cold plates, guard system surrounding the plates, temperature sensors, metal-sheathed heaters, and vacuum/gas pressurization system. An initial assessment of the calibration uncertainties for the primary measurement sensors is presented.