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Author
Sant, G. | Dehadrai, M. | Bentz, D. P. | Lura, P. | Ferraris, C. F. | Bullard, J. W. | Weiss, J.
Title
Detecting the Fluid-to-Solid Transition in Cement Pastes.
Coporate
Purdue Univ., West Lafayette, IN Tourney Consulting Group, Kalamazoo, MI National Institute of Standards and Technology, Gaithersburg, MD EMPA, Switzerland
Journal
Concrete International, Vol. 31, No. 6, 53-58, June 2009
Keywords
cements | cement pastes | construction | time | stress (mechanics) | structures | calorimetry | rheology | shrinkage
Identifiers
techniques sensitive to volume change; techniques sensitive to stress resistance or development; techniques sensitive to structure development; relating structure development to degree of reaction; chemical shrinkage; autogeneous shrinkage; Vicat test; ultrasonic testing; CEMHYD3D; cementitious materials
Abstract
The time of set for concrete is extremely important when scheduling construction operations. The fluid-to-solid transition that occurs during setting is crucial in assessing practical construction operations, such as finishing, sawcutting, and curing, and determining when test procedures such as early-age shrinkage measurements should be initiated. The solidification of cementitious mixtures can be identified using a variety of techniques. Each of the investigated techniques indicates that solidification occurs after a similar time period and contributes to a more detailed understanding of the fluid-to-solid transition. The interpretation of the results of each technique are described from a fundamental viewpoint, along with additional insight into the behavior of concrete that the techniques help explain or illustrate. Details of the investigated test methods can be found in a companion paper available with the online version of this article at www.concreteintemational.com.