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Author
Shaw, M. T. | Tobolsky, A. V.
Title
Thermal Stability of the Carbon-Carbon Crosslinkage in Polymer Networks.
Coporate
Princeton Univ., NJ
Sponsor
Office of Naval Research, Washington, DC
Report
ONR-TR-RLT-123
April 1970
20 p.
Distribution
Available from National Technical Information Service
Contract
N00014-67-A-0151-0011
Keywords
carbon | thermal stability | elastomers | silicones rubber | polyethylenes
Identifiers
chemical stress relaxation
Abstract
The thermal stability of carbon-carbon crosslinkages in elastomeric systems was studied by comparing the vacuum chemical stress relaxation of samples with different concentrations of these crosslinkages. The systems studied included silicone rubber, crosslinked polyethylenes and Dexsil-201 rubber. Arrhenius activation energies of about 55 kcal/mole were found for the scission of these crosslinkages in the temperature range 300-350 deg C. Crosslinkages added to a sample by additional curing were found to be, in general, more stable than those first formed.