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Author
Goldfarb, I. J.
Title
Kinetic Analysis of Thermogravimetry. Part 3. Experimental Modifications.
Coporate
Air Force Materials Lab., Wright-Patterson AFB, OH
Report
AFML-TR-68-181
September 1971
47 p.
Distribution
Available from National Technical Information Service
Keywords
thermogravimetry | kinetics | temperature measurements | magnetic tapes
Abstract
The experimental apparatus for temperature programmed thermogravimetry has been modified to more effectively obtain kinetic parameters for the degradation of polymers. The thermobalance was modified to incorporate direct sample temperature measurement thereby to minimize temperature measurement errors. An automatic data acquisition system was incorporated into the apparatus and appropriate computer programs to handle the magnetic tape data were written. The modified apparatus has been tested with several polymer systems and it was demonstrated that the use of the magnetic tape data recording sytem permitted greatly increased output from the thermobalance.